Matches in UGent Biblio for { <https://biblio.ugent.be/publication/1002928#aggregation> ?p ?o. }
Showing items 1 to 39 of
39
with 100 items per page.
- aggregation classification "A1".
- aggregation creator B191959.
- aggregation creator B191960.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation date "2010".
- aggregation format "application/pdf".
- aggregation hasFormat 1002928.bibtex.
- aggregation hasFormat 1002928.csv.
- aggregation hasFormat 1002928.dc.
- aggregation hasFormat 1002928.didl.
- aggregation hasFormat 1002928.doc.
- aggregation hasFormat 1002928.json.
- aggregation hasFormat 1002928.mets.
- aggregation hasFormat 1002928.mods.
- aggregation hasFormat 1002928.rdf.
- aggregation hasFormat 1002928.ris.
- aggregation hasFormat 1002928.txt.
- aggregation hasFormat 1002928.xls.
- aggregation hasFormat 1002928.yaml.
- aggregation isPartOf urn:issn:0021-9673.
- aggregation language "eng".
- aggregation publisher "Elsevier".
- aggregation rights "I have transferred the copyright for this publication to the publisher".
- aggregation subject "Veterinary Sciences".
- aggregation title "Development and validation of an ultra-high performance liquid chromatography tandem mass spectrometry method for quantifying thyreostats in urine without derivatisation".
- aggregation abstract "Thyreostatic drugs, illegally administrated to livestock for fattening purposes, are banned in the European Union since 1981 (Council Directive 81/602/EC). For monitoring their illegal use, sensitive and specific analytical methods are required. In this study an UHPLC-MS/MS method was described for quantitative analysis of eight thyreostatic drugs in urine, this without a derivatisation step. The sample pretreatment involved a reduction step with dithiothreitol under denaturating conditions at 65 degrees C, followed by liquid-liquid extraction with ethyl acetate. This analytical procedure was subsequently validated according to the EU criteria (2002/657/EC Decision), resulting in decision limits and detection capabilities ranging between 1.1 and 5.5 mu g L-1 and 1.7 and 7.5 mu g L-1, respectively. The method obtained for all, xenobiotic thyreostats, a precision (relative standard deviation) lower than 15.5%, and the linearity ranged between 0.982 and 0.999. The performance characteristics fulfill not only the requirements of the EU regarding the provisional minimum required performance limit (100 mu g L-1), but also the recommended concentration fixed at 10 mu g L-1 in urine set by the Community of Reference Laboratories. Future experiments applying this method should provide the answer to the alleged endogenous status of thiouracil. (c) 2010 Elsevier B.V. All rights reserved.".
- aggregation authorList BK451972.
- aggregation endPage "4293".
- aggregation issue "26".
- aggregation startPage "4285".
- aggregation volume "1217".
- aggregation aggregates 1002937.
- aggregation isDescribedBy 1002928.
- aggregation similarTo j.chroma.2010.04.030.
- aggregation similarTo LU-1002928.