Matches in UGent Biblio for { <https://biblio.ugent.be/publication/2025924#aggregation> ?p ?o. }
Showing items 1 to 33 of
33
with 100 items per page.
- aggregation classification "A1".
- aggregation creator person.
- aggregation creator person.
- aggregation date "2011".
- aggregation format "application/pdf".
- aggregation hasFormat 2025924.bibtex.
- aggregation hasFormat 2025924.csv.
- aggregation hasFormat 2025924.dc.
- aggregation hasFormat 2025924.didl.
- aggregation hasFormat 2025924.doc.
- aggregation hasFormat 2025924.json.
- aggregation hasFormat 2025924.mets.
- aggregation hasFormat 2025924.mods.
- aggregation hasFormat 2025924.rdf.
- aggregation hasFormat 2025924.ris.
- aggregation hasFormat 2025924.txt.
- aggregation hasFormat 2025924.xls.
- aggregation hasFormat 2025924.yaml.
- aggregation isPartOf urn:issn:0306-7319.
- aggregation language "eng".
- aggregation rights "I have transferred the copyright for this publication to the publisher".
- aggregation subject "Medicine and Health Sciences".
- aggregation title "Determination of four basic pharmaceuticals and one pesticide in surface water with UPLC-ESI-MS/MS".
- aggregation abstract "This paper describes the optimisation and validation of an ultra performance liquid chromatography- tandem mass spectrometry (UPLC-MS/MS) method for the analysis of four pharmaceuticals (flubendazole, pipamperone, rabeprazole and domperidone) and one pesticide (propiconazole) in surface water. Sample preparation was reduced substantially as compared to a previously published high performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) method, thanks to the use of UPLC. In addition, internal standards could now be used for quantification instead of the standard addition method. Extraction was performed on a Speedisk phenyl solid-phase extraction tube. A Waters Acquity HSS T3 UPLC column (100 x 2.1mm i.d.; 1.8-mu m particles) was used for separation and an API 4000 triple quadrupole was used as a detector. Total run time was 8.59 minutes. Matrix effects were examined on different surface water samples. Limits of detection and quantification in surface water samples were between 100 and 500 pg/l. Validation was performed on surface water. The method showed good precision (<15%) and accuracy (85-120%). This method is less time-consuming and labour-intensive than a previously published HPLC-procedure without compromising validation parameters.".
- aggregation authorList BK486518.
- aggregation endPage "1226".
- aggregation issue "12".
- aggregation startPage "1218".
- aggregation volume "91".
- aggregation aggregates 2025932.
- aggregation isDescribedBy 2025924.
- aggregation similarTo 03067311003778664.
- aggregation similarTo LU-2025924.