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- aggregation classification "A1".
- aggregation creator B375102.
- aggregation creator B375103.
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- aggregation date "2012".
- aggregation format "application/pdf".
- aggregation hasFormat 3047623.bibtex.
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- aggregation isPartOf urn:issn:1463-9076.
- aggregation language "eng".
- aggregation rights "I have transferred the copyright for this publication to the publisher".
- aggregation subject "Chemistry".
- aggregation title "Synthesis, characterization and sorption properties of NH₂-MIL-47".
- aggregation abstract "An amino functionalized vanadium-containing Metal Organic Framework, NH2-MIL-47, has been synthesized by a hydrothermal reaction in an autoclave. Alternatively, a synthesis route via microwave enhanced irradiation has been optimized to accelerate the synthesis. The NH2-MIL-47 exhibits the same topology as MIL-47, in which the V center is octahedrally coordinated. After an exchange procedure in DMF the V+III center is oxidized to V+IV, which is confirmed by EPR and XPS measurements. The CO2 and CH4 adsorption properties have been evaluated and compared to MIL-47, showing that both MOFs have an almost similar adsorption capacity and affinity for CO2. DFT-based molecular modeling calculations were performed to obtain more insight into the adsorption positions for CO2 in NH2-MIL-47. Furthermore our calculated adsorption enthalpies agree well with the experimental values.".
- aggregation authorList BK677328.
- aggregation endPage "15570".
- aggregation issue "44".
- aggregation startPage "15562".
- aggregation volume "14".
- aggregation aggregates 3050748.
- aggregation isDescribedBy 3047623.
- aggregation similarTo C2CP42137B.
- aggregation similarTo LU-3047623.