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- aggregation classification "A1".
- aggregation creator B224384.
- aggregation creator B224385.
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- aggregation date "2013".
- aggregation format "application/pdf".
- aggregation hasFormat 3182996.bibtex.
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- aggregation isPartOf urn:issn:0340-4285.
- aggregation language "eng".
- aggregation rights "I have transferred the copyright for this publication to the publisher".
- aggregation subject "Chemistry".
- aggregation title "Dioxygen activation in photooxidation of diphenylmethane by a dioxomolybdenum(VI) complex anchored covalently onto mesoporous titania".
- aggregation abstract "A dioxomolybdenum(VI) complex has been covalently anchored onto mesoporous titania by a silicon-assisted transesterification route. The grafting of the complex to the mesoporous structure was confirmed by diffuse reflectance infrared Fourier transform, Raman and UV-Vis spectroscopy and by nitrogen sorption experiments. The ability of the grafted complex to activate molecular oxygen (O-2) has been evaluated in the photooxidation of diphenylmethane to produce benzophenone. The photooxidation of diphenylmethane was monitored continuously by in situ dispersive Raman spectroscopy. A scheme for the activation of molecular oxygen under very mild conditions is proposed. A comparison with the same complex anchored onto commercial titanium P-25 and silica gel revealed both the beneficial effect of the mesoporous structure and the existence of a synergistic effect between MoO/TiO2/O-2/light entities, which promotes the photooxidation process under green chemistry conditions. Finally, the heterogeneous catalyst is sustainable; it can be recycled and reused without significant loss in activity or selectivity.".
- aggregation authorList BK491415.
- aggregation endPage "127".
- aggregation issue "2".
- aggregation startPage "119".
- aggregation volume "38".
- aggregation aggregates 3183009.
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- aggregation similarTo s11243-012-9668-2.
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