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- aggregation classification "A1".
- aggregation creator B866768.
- aggregation creator B866769.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation date "2013".
- aggregation format "application/pdf".
- aggregation hasFormat 4096076.bibtex.
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- aggregation isPartOf urn:issn:1875-0710.
- aggregation language "eng".
- aggregation rights "I have transferred the copyright for this publication to the publisher".
- aggregation subject "Chemistry".
- aggregation title "Rapid and sensitive LC-MS/MS determination of ergot alkaloids in buffered solutions: application to in vitro testing of a clay-based mycotoxin binder".
- aggregation abstract "A rapid liquid chromatography-tandem mass spectrometric (LC-MS/MS) method was developed for the determination of ergot alkaloids in buffered solutions from in vitro studies. The method implied a liquid-liquid extraction of the analytes under alkaline conditions prior to LC-MS/MS analysis and resulted in good recovery (91-123%) of the six ergot alkaloids defined by the European Food Safety Authority as most important, namely ergometrine, ergosine, ergotamine, ergocornine, ergokryptine and ergocristine, as well as their corresponding epimers. The method also proved to be sensitive, repeatable, linear, accurate and robust. Furthermore, the method was applied to evaluate the in vitro binding efficacy of a clay-based mycotoxin binder towards ergometrine, ergosine and ergocornine, through a design encompassing pH 3.0 and 6.8 to mimic the digestive tract. The binder demonstrated binding efficacy of 24, 93 and 97%, respectively, for these ergot alkaloids.".
- aggregation authorList BK1244338.
- aggregation endPage "115".
- aggregation issue "2".
- aggregation startPage "105".
- aggregation volume "6".
- aggregation aggregates 4096090.
- aggregation isDescribedBy 4096076.
- aggregation similarTo WMJ2012.1528.
- aggregation similarTo LU-4096076.