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- aggregation classification "A1".
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation creator person.
- aggregation date "2009".
- aggregation format "application/pdf".
- aggregation hasFormat 740327.bibtex.
- aggregation hasFormat 740327.csv.
- aggregation hasFormat 740327.dc.
- aggregation hasFormat 740327.didl.
- aggregation hasFormat 740327.doc.
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- aggregation isPartOf urn:issn:1022-1336.
- aggregation language "eng".
- aggregation publisher "WILEY-V C H VERLAG GMBH".
- aggregation subject "Chemistry".
- aggregation title "‘Click’ functionalization of cryogels conveniently verified and quantified using high- resolution MAS NMR spectroscopy".
- aggregation abstract "Chemical modification reactions of alkyne containing polyHEMA-based macroporous network structures (cryogels) by Cu(I) catalyzed azide-alkyne 'click' cycloaddition reactions and their monitoring and quantification with high-resolution magic angle spinning (hr-MAS) NMR spectroscopy are reported. Complete conversion is obtained when benzylazide is reacted with the grafted alkyne function, but only partial conversion is observed when using azide-modified poly(ethylene glycol) (PEG-N-3). Subsequent addition of benzylazide consumes all remaining alkyne groups. All chemical modifications are easily monitored at each stage using hr-MAS NMR spectroscopy. The alkyne functionality and the resulting triazole ring provide well resolved H-1 resonances to monitor and quantify the progress of such 'click' reactions in general.".
- aggregation authorList BK687783.
- aggregation endPage "1333".
- aggregation issue "15".
- aggregation startPage "1328".
- aggregation volume "30".
- aggregation aggregates 741971.
- aggregation isDescribedBy 740327.
- aggregation similarTo marc.200900087.
- aggregation similarTo LU-740327.